| 摘要: |
| 采用高效液相色谱（HPLC）法测定无盐咪唑啉中丙烯酸的含量。结果表明，丙烯酸在9.09
～77.27 μg/mL与峰面积有良好的线性关系（r =0.999 5），该方法的检出限和定量限分别为0.1 μg/mL
和0.3 μg/mL；精密度、重复性实验相对标准偏差（RSD）均小于2.0%。丙烯酸的平均加标回收
率为90.99%，RSD为2.52%(n =9)。 |
| 关键词: 无盐咪唑啉 丙烯酸 高效液相色谱 |
| DOI： |
| 分类号: |
| 基金项目: |
|
| Determination of acrylic acid in salt-free imidazoline by high performance liquidchromatography |
|
MA Li-na
|
|
Shanghai Fine Chemical Co., Ltd.,
|
| Abstract: |
| The content of acrylic acid in salt-free imidazoline was determined by high performance liquid chromatography. The results
showed that the linear range of acrylic acid was 9.09 ~ 77.27 μg/mL (r = 0.999 5), the LOD was 0.1 μg/mL and the LOQ was 0.3 μg/mL.
The RSD of precision and reproducibility tests were both less than 2.0%. The average recovery of the acrylic acid was 90.99%, and the
RSD was 2.52% (n=9). |
| Key words: salt-free imidazoline acrylic acid high performance liquid chromatography |
